Fig. 1 shows the simultaneous DSC/TGA curves of the complex precursor for CCTO-1 measured at a heating rate of 10 °C min −1 in air. The TGA curve shows a minor weight loss step between 30 and 200 °C, which is related to the losses of moisture, hydrate decomposition and trapped solvent (water and carbon dioxide).A major weight loss is observed between 250 and 400 °C, and there is almost no ...
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